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Troubleshooting Guide — Gas Sampling - NOA 280i


A list of possible problems with the chemiluminescence detector appears below. If the problem is not listed below or assistance is needed, contact GE Analytical Instruments.

Gas Calibration outside recommended limits
 Possible Causes
Action Required
NO gas concentration low due to absorption in regulator Allow cal gas to flow for at least 5 minutes before calibrating
Cal gas flow rate too low(no flow out open leg of tee) Increase cal gas flow rate to > 250 mL/min
Dirty/clogged frit restrictor Clean or replace the frit restrictor
Dirty filter Replace Teflon filter in gas sampling line
Dirty Reaction chamber Cleanreaction chamber
High voltage needs adjustment Contact GE Analytical Instruments
 
Zero Air Calibration outside recommended limits
Possible Causes
Action Required
Leak at zero air filter Confirm all connections are tight
No flow through zero air filter Insure caps are removed from both ends of zero air filter.
Light Leak See PMT test in Detector Problems troubleshooting section.
Cooler Temperature too high Allow at least 30 minutes after turning power on before calibrating.
Perform cooler maintenance if necessary.
 
High Background after NO calibration
Possible Causes Action Required
Dirty Teflon filter Replace the filter

 

NOA 280i (startpage)

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