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Flash kolonner fra Interchim

  interchim

puriFlash kolonner /columns

High Performance & High Capacity Columns

puriFlash HP, High Performance

Spherical silica has superior flow properties when
compared to irregular shaped, flash grade silica.
PuriFlah HPcolumns are packed with either 15,
30 or 50µ spherical silica. Columns are available
from 4g to 1.6kg and are compatible with any flash
system.

 

puriFlash HC, High Capacity

PuriFlash HC, is the big brother of puriFlash HP. It is an ultra-high surface area silica. When it comes to large scale purification, loading is a critical factor. The example below shows that purity is easily achieved with a 20% sample load. Available in bulk and all column sizes from 4g to 1.6kg.

PuriFlash High Performance & High Capacity Columns
Column Selection Guidelines
Silica Grade Particle Size Suggested Use
50SIHC 50µ Every Day Use, High Capacity
50SIHP 50µ Every Day Use
30SIHP 30µ When you need a little Oomph*
15SIHP 15µ Guaranteed Separation

* Oomph: Vigor, liveliness, get up and go.

 

Fig Column Part number Flow Pressure Gradient profile Sample
injection
Sample
load, g
Sample
load, %
1 40-60µ irregular SI, 25g IR-50SI/25G
20 ml/min
15 psi
0-9.6: 0-20% B
2 ml
1 g
4%
2 15µ puriFlash Si HP,25g PF-15SIHP/25G
40 mil/min
30 psi
0-4.8: 0-20% B,
4.8-5.6: 20% B
2 ml
1 g
4%
3 50µ puriFlash SiHc,25g PF-50SIHC/25G
20 ml/min
7 psi
0-4.8: 0-20% B,
4.8-6.4: 20% B
10 ml
5 g
20%

Test Conditions: A (Hexane B), B (Ethyl acetate), 254nm. 500mg/ml. Dimethyl phthalate, Diethyl phthalate, Dibutyl phthalate

 

 

puriFlash HP columns

Speed AND Resolution. Have it All with PuriFlash HP Columns!

With puriFlash HP columns, speed and resolution are achieved by using spherical silica, steeper gradients and higher flow rates without increased backpressure. Flash purification is now 3x faster!

  • See the difference!Save time by collecting fewer fractions
  • Faster throughput via higher flow rates
  • Reduce solvent consumption
  • 15µ for difficult separations
  • Lower pressure with spherical silica
  • 30 bonded phases; reverse phase,
    ion exchange and more!
  • Use on ANY flash system

puriFlash offers faster throughput via higher flow rates

High Speed Columns - PuriFlash

Interchim provides columns packed with highly efficient spherical silica.
The 15µ and 30µ columns improve resolution and reduce run times by up to 70%
.

Spherical silica has superior flow properties when compared to irregular shaped, flash grade silica. As a general rule, 30µ puriFlash and 40-60µ flash grade silica have similar pressure values.

PuriFlash columns are packed with either 15, 30 or 50µ particles. Columns are available from 4g to 1.6kg and are compatible with any flash system.

Download flash column brochure

High Throughput system (puriFlash 430evo instrument)

PuriFlash columns are compatible with any manufacturers’ system. The high pressure rating ensures optimum performance when using increased flow rates with smaller particles. Columns are available in liquid injection and dry-load formats.

  • 15µ, 30µ or 50µ Spherical Silica
    Spherical silica and smaller particles greatly improve separation efficiency
  • Stable to 20 bar / 300 psi
    Work at higher flow rates
  • 40 Bonded Phases
    Choose from over 40 phases for reverse
    phase, normal phase, ion exchange, mixed
    mode and chiral

 

puriFlash HC columns

5x Higher Load Capacity with puriFlash HC

Test Conditions: A: cyclohexane B: ethyl acetate; Gradient: 0-10:00, 0-30% B, hold at 30%;
Sample concentration: 250 mg/ml; Sample: diethyl phthalate, dimethyl phthalate

Higher Loading, Twice as Fast, Lower Cost

PuriFlash HC, high capacity flash columns, use an ultra-high surface area silica which provides two times the sample loading when compared to conventional flash silica. For large scale purification, puriFlash HC is the obvious choice. In the example shown above, a 300g puriFlash HC column provided superior results when compared to a 600g conventional flash column.

PuriFlash HC is available in bulk and in column sizes from 4g - 1600g.

 

Fig Column Part number Flow Pressure Gradient profile Sample
injection
Sample
load, g
Sample
load, %
1 40-60µ irregular SI, 25g IR-50SI/25G
20 ml/min
15 psi
0-9.6: 0-20% B
2 ml
1 g
4%
2 50µ puriFlash Si HP,25g PF-50SIHP/25G
20 ml/min
7 psi
0-4.8: 0-20% B,
4.8-65.6: 20% B
2 ml
1 g
4%
3 30µ puriFlash Si HP,25g PF-30SIHP/25G
30 ml/min
15 psi
0-4.8: 0-20% B,
4.8-5.6: 20% B
2 ml
1 g
4%
4 15µ puriFlash Si HP,25g PF-15SIHP/25G
40 mil/min
30 psi
0-4.8: 0-20% B,
4.8-5.6: 20% B
2 ml
1 g
4%


  Test Conditions: A (Hexane B), B (Ethyl acetate), 254nm. 500mg/ml. Dimethyl phthalate, Diethyl phthalate, Dibutyl phthalate

 

 

 

For flere detaljer og pris, kontakt venligst MD Scientific via e-mail: info@md-scientific.dk eller telefon: 7027 8565.

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MD Scientific
MD Scientific
MD Scientific
MD Scientific ApS • Denmark • tlf. 7027 8565 • fax 7027 8566 • info@md-scientific.dk